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Editor's Note: This content was originally published in USA Today

The flow rate for each run started at 0.2 ml/min for 5 min, followed by a gradient starting at 0% B and increasing linearly to 100% B over the course of 45 min with a flow rate of 0.7 ml/min, followed by an isocratic gradient of 100% B for 17 min at 0.7 ml/min before equilibrating for 8 min at 0% B with a flow rate of 0.7 ml/min

Don Catlin, worked to identify and expose these substances leading to one of the largest anti-doping scandals ever with the BALCO affair in 2002