Pharm Res 41 , 19912014 (2024)
Clauw DJ 1 EULAR revised recommendations for the management of fibromyalgia [PubMed Abstract] [Full Text HTML] [Full Text PDF]
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After the reaction, concentrate the reaction solution under reduced pressure, add DCM to redissolve, wash with saturated brine three times, put the collected DCM solution into a certain amount of anhydrous sodium sulfate for drying, let it stand for 0.5 hours, suction filter, and collect the filtrate After pumping to dryness, 1.89 g of crude compound 0 was obtained, which was set aside
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