200L of a 50:50 water: acetonitrile solution with 10% formic acid was added to each tube and centrifuged at 13,500 rpm for 5 minutes
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Oakeshott JG, Johnson RM, Berenbaum MR, Ranson H, Cristino AS, Claudianos C
Other companies have been prosecuted for causing false claims to be submitted because of the companies marketing of the product for unapproved, and thus generally non-reimbursable, uses and purportedly concealing price concessions in the pricing information submitted to the government for government priced reporting purposes
NCBI Bookshelf [2] Kommu, S., & Whitfield, P